Rey

Bruker AVIII-HD 700 (solution and solid-state NMR)

Available Probes: 

Ultra-high sensitivity 5mm TCI helium temperature cryoprobe. 1H observe with 15N and 13C decoupling. 13C observe with 1H and 15N decoupling including 2H decoupling.  The probe includes actively shielded Z gradients with automatic tuning and matching. Variable temperature from -40 to +80 °C. Although this probe can run all types of standard 1H and 13C NMR samples, it is optimized for multi-dimensional biological samples.

700 MHz 5mm broadband probe for 1H, 15N – 31P with actively shielded Z gradients and automatic tuning and matching. Variable temperature from -150 to +150 °C.

E-free triple resonance 13C/15N/1H  MAS probe for 3.2 mm o.d. rotors. The maximum MAS speed is 24 kHz. Variable temperature from -80 to 80 oC.

Double resonance low-gamma MAS probe for 4 mm o.d. rotors. The maximum MAS speed is 15 kHz. Tuning range: 1H, 109Ag – 27Al.  Variable temperature from -30 to +70 oC.

Double resonance HX very-fast MAS probe for 1.3 mm o.d. rotors. The maximum MAS speed is 65 kHz. Tuning range: 1H, 15N – 31P.  Variable temperature from -30 to +70 oC.

Accessories: 

Case 24 sample auto-sampler under the control of ICONNMR software.

BCU-1 temperature stabilization accessory.

Applications:

Extremely sensitive NMR study of complex molecules in solution.

Solid-state NMR of biomolecules or quadrupolar nuclei.